RUTHENIUM CARBONYL CAS#: 15243-33-1

IdentificationPhysical DataSpectraRoute of Synthesis (ROS)Safety and HazardsOther Data Identification Product NameRUTHENIUM CARBONYLMolecular StructureCAS Registry Number 15243-33-1MDL NumberMFCD00011209Molecular FormulaC5H6N2Molecular Weight94.116 Physical Data SolubilityIt is soluble in water as well as soluble in alcohol, benzene. Melting Point, °C 144 - 145154 - 155154 - 156 Density, g·cm-3Measurement Temperature, °C2.56-173.162.552-173.162.552-153.162.486 Spectra Description (NMR Spectroscopy)Nucleus (NMR Spectroscopy)Solvents (NMR Spectroscopy)Temperature (NMR Spectroscopy), °C Frequency (NMR Spectroscopy), MHzSpectrum13CChemical shifts, Spectrum13Cbenzene-d6100.6Spectrum, Linewidth of NMR absorptionotherneat (no solvent, solid phase)othertetrahydrofuran39.84Spectrum13Cnot given Description (IR Spectroscopy)Solvent (IR Spectroscopy)Intensity of IR bands, Bands, Spectrumpotassium bromideBandsn-heptaneBandshexane Description (UV/VIS Spectroscopy)Solvent (UV/VIS Spectroscopy)Reflection spectrum, SpectrumSpectrumBand assignment, Spectrumethyl acetateSpectrumdichloromethane Route of Synthesis (ROS) Route of Synthesis (ROS) of Ruthenium carbonyl CAS 15243-33-1 ConditionsYieldWith triethylamine In propan-1-ol; water at 85℃; under 2625.26 Torr; Concentration; Reagent/catalyst; Solvent; Temperature; Pressure; Autoclave;Experimental ProcedureGeneral procedure: 10031] In this embodiment, a synthesis test to confirm the presence or absence of the effect by the addition of an amine to the reaction system for DCR synthesis was performed. The production process of DCR is as follows. Ruthenium chloride (manufactured by Tanaka Kikinzoku Kogyo K. K., ruthenium chloride content: 38.67 wt %, chlorine content: 47.4 wt %) and 1 -propanol were mixed and stirred to prepare a ruthenium chloride solution, and this was introduced into an autoclave (made of steel) having a capacity of 100 ml of the reaction vessel. Thereafier, an amine was added into the reaction vessel and further carbon monoxide was air tightly introduced into the reaction vessel until to have a predetermined reaction pressure. Thereafter, the temperature was raised to the reaction temperature while maintaining the predetermined reaction pressure with carbon monoxide, and the synthesis reaction of DCR was allowed to proceed. The solution was stirred during the reaction. The reaction conditions in the present embodiment were as follows. In the present embodiment, DCR was synthesized using a plurality of amines which has different numbers of carbon atoms. In addition, the possibility of the synthesis of DCR in the case of not adding an aminewas also investigated; The relation between the water content of 1-pro-panol before being used for the preparation of the rutheniumchloride solution and the yield of DCR was investigated. Theproduction process of DCR other than this was the same as inthe first embodiment. The reaction conditions were as follows. The measurement results of the yield of DCR in this testare shown in Table 5.10090] Ruthenium chloride: 1.58 g (Ru: 0.61 g)10091] 1 -propanol: 60 mE (water content: dry, 0.5 wt %, 1.0wt%, 3.Owt%, 5.Owt%, lOwt%and3owt%)10092] Triethylamine: 1.3 equivalents (molar equivalentwith respect to chlorine)10093] Reaction pressure: 0.35 MPaj0094]j0095]j0096]Reaction temperature: 85° C.Reaction time: 10 to 60 hoursStirring speed: 300 rpm. As can be seen from Table 5, there is a possibility that the yield of DCR is affected by the water content in the solvent. Moreover, it is not possible to obtain a practical yield of DCR in the case of using a solvent which contains water at 10% or more. From this fact, it is preferable to set the water content in the solvent to 5% by mass or less. However, it is not intended to require a dry state (water content of approximately 0%), and it is possible to obtain a high yield using a solvent having a water content of 1% or less.92.5%In methanol at 125℃; under 48754.9 Torr; for 8h; Autoclave; Safety and Hazards No data available Other Data No data available DruglikenessLipinski rules componentMolecular Weight639.335logPHBA12HBD0Matching Lipinski Rules1Veber rules componentPolar Surface Area (PSA)0Rotatable Bond (RotB)0Matching Veber Rules2 Use PatternRUTHENIUM CARBONYL is often used as a catalyst in organic synthesis. It facilitates the reaction between carbon monoxide and organic compounds, leading to the production of carbonyl compounds. These reactions are significant in the synthesis of pharmaceuticals and other organic compounds. And RUTHENIUM CARBONYL can also be employed as a catalyst in hydrogen transfer reactions, participating in reactions that enable the effective transfer of hydrogen in organic synthesis. Read the full article

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Anagram: A Discussion of (P)ublic (R)elations in the (R)epublic of the (P)hilippines

This is an article review for "Colonial and Other Influences in the History of Public Relations in the Philippines" by Sison et al (2011). This essay was written in partial fulfillment for my SPCM154 (Speech Communication in Public Relations) course.

In the age of social media, the role of public relations in maintaining brand images appears to be more prominent than ever. It may seem that the sudden influx of these companies’ attention to their brand image through various public relation stunts is due to the advancements of technology and new media. However, the field of public relations in the Philippines is so ingrained into our societal consciousness that most do not even fully recognize it. This is what authors Marianne Sison, Zeny Sarabia-Panol, Caterina Lorenzo-Molo and Ritzi Villarico-Ronquillo discuss in their journal article entitled ‘Colonial and other influences in the history of public relations in the Philippines’, a study they presented at Bournemouth University in the United Kingdom at The Proceedings of the International History of Public Relations Conference back in 2011. 

The target audience of the study is not intended towards Filipinos, but to a more global audience. It aimed to analyze how our concept of public relations is rooted in Philippine history, specifically in our colonial influences. The authors presented an extremely thorough account of the nation’s narrative as victims of imperialism from countries like the United States, Japan, and Spain. Since it was presented during a conference discussing how the individual histories of each nation impacted their respective public relations, their analysis is highly relevant to their target audience.

As stated before, the article first chronicles Philippine history meticulously, beginning from the colonization of the Spaniards alongside the introduction of Christianity to the invasion of Japan and the triumph of finally declaring our independence as a nation. It also briefly mentions the dark days of the Marcos regime and the 1986 People Power Revolution.

Afterward, the authors start to analyze the role of colonialism in public relations. Their main thesis revolves around the impact of our colonial influences in many aspects of business and political environments — which is ultimately where public relations come into play. Religion in particular has a very keen relationship with the world of PR, followed by journalism and education, and development communication. In fact, they even mention the University of the Philippines Los Banos as a pioneer in the field of development communication. They conclude with the sentiment that “Filipino public relations practitioners have to juggle between their Eastern culture, their Spanish-inspired religiosity, and their Americanized education within the context of a globalized economy. Despite a western approach to public relations, the Philippines is revealing its own brand of public relations that combines elements of the Eastern approach” (272). 

The authors came to this conclusion through a thorough and meticulous understanding of the Philippine context, along with an analysis of how public relations is rooted in different fields. Their methodologies do not include any new statistical data to back their claims; instead, they opt for a more qualitative approach using related literature to support their thesis. The structure of the article is even structurally significant to that of a standard review of related literature.

Overall, the article is a very compelling read. It really puts the relationship of the Philippines’ history and public relations into perspective and invokes readers to question their understanding of modern public relations, especially in this age where brand imagery plays a large role in shaping the consciousness of the masses. The writing style is easy to comprehend, which is important considering the fact that their target audiences are from diverse backgrounds and cultures. Overall, they manage to emphasize their main points, especially in the conclusions they arrive at. Their usage of Philippine history as a main evidence to support their thesis is also an effective decision. It can even be a testament to some of the more positive impacts of colonization to our country’s development, especially considering the fact that our public relations opened us to the world of foreign or global trade and having good ties with neighboring countries. 

Personally, I believe the textual evidence is enough to support the authors’ main claim. It is hard to argue the fact that Filipinos do experience an amalgam of cultural nuances within our own societal consciousness, and public relations is a very big aspect of that. Public relations is in everything we do — we are saturated in a capitalist world that thrives on consumerism and relations. My only qualms with the article itself is perhaps the over-meticulousness of how they detailed the history of the Philippines. It is understandable that a thorough understanding of this is key to properly linking the evidences they presented to the main thesis they are arguing, but in the context of an audience that is mainly non-Filipino who have been exposed to a variety of cultures, it may be a bit too overwhelming or disinteresting at some points in the article. 

However, overall, the article effectively highlights the relevance of Philippine history and public relations and comes to a well-researched and satisfying conclusion. It proves itself as a relevant piece because it uses the past to explain the present while also giving us the perception of how the future will be. It changes one’s paradigm and compels us to ask questions about our history and what other implications it brings about in modern day society. Most of all, it brings public relations into a new light and challenges its audiences to rethink our perception of the world of public relations in the Philippines. 

Reference: Marianne Sison, PhD, Zeny Sarabia-Panol, PhD, Caterina Lorenzo-Molo, PhD, & Ritzi Villarico-Ronquillo. “Colonial and other influences in the history of public relations in the Philippines.” The Proceedings of the International History of Public Relations Conference. Bournemouth University, 2011. 265 – 275 pp. 

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